Artemis (av400) rules
- Do not remove sample # 96: 30mg sucrose in D20.
- Discard old caps, and any tubes or caps that are damaged in any way. Norell caps should not be used > 10 times, Bruker > 3 times.
- Do not use Norell caps and Wilmad WG-1000 tubes.
- Multiple sample submissions:
Submit no more than 3 samples to the dayqueue. All other samples must go into the nightqueue.
— dayqueue limits: 12 min max/exp; 20 min total/day; 18 min max dropdown
- Nightqueue submissions:
Take ≤ 2 hr total time when submitting before 10 pm.
After 10 pm, you may use all remaining nightqueue time.
Callisto (av500) rules
- Night queue submissions:
–> Each user is allowed an unlimited amount of night queue time. But when submitting before 10pm (7pm weekends), use up to or less than 3 hr total (not per sample, but total time per user). This rule gives other users time to get their samples done.
–> If you need to perform long experiments, talk to NMR staff.
- Callisto is very sensitive to pH (keep between 4 and 8) and salt concentration (stay below 100 mM). Please talk to NMR staff if you are unsure about your sample.